AssayIndex

AX-2026-041557

GHRP-6 · 5 mg declared · Qingdao Sigma Chemical Co., Ltd. · lot QSC-2605-A6715

PASSIDENTITY CONSISTENT
Report ID
AX-2026-041557
Compound
GHRP-6
Compound class
Growth-hormone axis peptides
Supplier
QSC — Qingdao Sigma Chemical Co., Ltd.
Batch / lot
QSC-2605-A6715
Declared label claim
5mg
Laboratory
Medutest
Assay date
29 Apr 2026
Submitted
10 May 2026
Quarter
2026-Q2
Submitter
j.roos
Sample provenance
Buyer-sourced
Section 1

Results

Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.

ParameterMethodResultUnitIndex spec
PurityRP-HPLC, 25 min gradient, 214 nm99.73% area≥ 99.0PASS
Total impuritiesRP-HPLC, sum of reported peaks0.27% area≤ 1.0PASS
Largest single impurityRP-HPLC — bis-oxidised Trp (+32 Da)0.14% area≤ 1.00PASS
Identity — theoretical monoisotopic masscalculated from molecular formula872.4446DaNOT TESTED
Identity — observed monoisotopic massLC-MS, unit resolution (single quadrupole)872.4511DaNOT TESTED
Mass accuracyobserved vs theoretical+7.5ppm± 15PASS
Total peptide contentby difference from the gravimetric mass balance90.75%w/wNOT TESTED
Target-compound contenttotal peptide content × purity90.50%w/wNOT TESTED
Gross fill (as weighed)five-place balance, under nitrogen5.22mg5 mg declaredNOT TESTED
Recovered target peptidegross fill × target content4.724mg5 mg claimNOT TESTED
Recovery against label claimrecovered ÷ claim94.5%90.0 – 110.0PASS
Water contentKarl Fischer, coulometric, duplicate4.88%≤ 9.0PASS
Counter-ion (acetate)anion-exchange ion chromatography4.17%≤ 12.0PASS
Residual solvent + inorganic residueestimated — see /methods/residual-solvents-q3c/0.20%NOT TESTED
Endotoxinnot ordered on this submissionnot determined≤ 5.0NOT TESTED
Sterilitynot ordered on this submissionnot determinedno growthNOT TESTED
Appearancevisual, diffuse light, black and white backgroundWhite lyophilised cake, intactwhite to off-white intact cakePASS
Reconstitution clarityreconstituted per submitter procedureClear, colourless, no visible particulatesclear, no visible particulatesPASS
pH (reconstituted, 1 mg/mL)potentiometric, two-point calibration5.642.5 – 8.0PASS
Retention time (observed)RP-HPLC, 25 min gradient7.20min7.15 ± 0.25 (normalised)PASS
Peak asymmetry (10 % height)Ph. Eur. 2.2.460.950.80 – 1.50PASS
Plate count, main peakN = 5.54 (t/w½)²69,700≥ 20,000PASS
Resolution to nearest impurityvs [D-Trp]-epimer0.89no index criterionREPORTED
Section 2

Chromatogram and peak integration

The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.

0434286831302517366 GHRP-67.20 min · 99.73 % 6.72 same trace · ×200 vertical expansion, baseline-corrected · main peak off-scale reporting threshold 0.05 % area 0481216202428 Retention time (min) Response (mAU)
Figure 1. RP-HPLC trace, 25 min gradient, 214 nm. Drawn from the peak-integration table below: peak positions are the reported retention times, peak areas are the reported area percentages, peak widths follow the reported plate count of 69,700, and skew follows the reported asymmetry factor of 0.95. Baseline noise is seeded from the report ID and is illustrative. The lower panel is the same trace at a stated vertical expansion with the slow gradient drift subtracted, because at full scale a 0.14 % impurity against a 99.73 % main peak is a line two pixels tall; the main peak runs off-scale there by design.
#PeakRTArea (µV·s)% areaΔ mass (Da)
1GHRP-6 — main peak7.204,847,18799.73
2bis-oxidised Trp (+32 Da)6.726,8040.14+31.990
3oxidised Trp (+16 Da)6.924,3740.09+15.995
4[D-Trp]-epimer7.109720.020.000
5des-Lys (−128 Da)7.029720.02-128.095
Closure check — purity + Σ impurities 100.00CLOSES

Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.

Section 3

Mass spectrum and identity

Theoretical monoisotopic mass 872.4446 Da, computed from C46H56N12O6. All ppm figures on this site are against monoisotopic values — see why that matters.

0255075100375475575675775875975 [M+1H]1+873.46[M+2H]2+437.23 m/z Relative abundance (%)
Figure 2. ESI charge-state envelope, unit-resolution instrument. Sticks are placed at m/z = (M + z × 1.007276)/z for the observed neutral mass of 872.4511 Da. Sodium (+21.982/z) and potassium (+37.956/z) adducts are shown where the parent charge state exceeds 25 % relative abundance; they are adducts of the same molecule and are not impurities.
ChargeTheoretical m/zObserved m/zΔ m/zRel. abundance (%)
2+437.2296437.23280.003254.4
1+873.4519873.45840.0065100.0
Section 4

Gravimetric mass balance

Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.

ComponentDetermination%w/w of cake
WaterKarl Fischer4.88
Counter-ion (acetate)ion chromatography4.17
Residual solvent + inorganic residueestimated0.20
Total peptide contentby difference90.75
Total100.00 CLOSES

Supplier certificate, as declared

The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.

FigureSupplier COAThis reportIndex note
Purity (% area)99.7299.73divergence -0.04 pp vs batch median
Total impurities (% area)0.280.27
Largest single impurity (% area)0.150.14
Water (%)not stated4.88
Counter-ion (%)not stated4.17
Peptide content (%w/w)91.790.75
Endotoxin (EU/mg)not statednot determined
Method stated on certificateYEScolumn, gradient and wavelength given
Section 5

Provenance and caveats

Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.

Sample provenance
Buyer-sourced
Evidentiary weight
Strongest available evidence in this index.
Chain of custody
Retail purchase → submitter (2–8 °C, 33 d) → laboratory (courier, ambient, 11 d) → assay.
Assay date
29 Apr 2026
Submitted to the index
10 May 2026
Laboratory
Medutest, Ljubljana, Slovenia
Method basis
25 min gradient · unit-resolution MS
Verification status
IDENTITY CONSISTENT
Section 6

Annotations 2

Signed technical comments from index contributors. Not a discussion forum — annotations question or contextualise the result, and the data team replies where a reply is warranted.

lot_traceability
Lot QSC-2605-A6715 on the vial matches the certificate that came with it. That is the check every buyer can do in ten seconds and most do not.
coa_template
The document that arrived with this order is on file and its fields are scored on the supplier's documentation rubric. That score describes what a buyer receives, which is the useful version.
Section 7

Related records

Same batch — lot QSC-2605-A6715 n=10

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-041548QSC-2605-A6715Janoshik2026-Q299.715.0788.7Buyer-sourced1MARGINAL
AX-2026-041549QSC-2605-A6715Medutest2026-Q299.934.83Buyer-sourced0PASS
AX-2026-041550QSC-2605-A6715Janoshik2026-Q299.775.00101.8Buyer-sourced0PASS
AX-2026-041551QSC-2605-A6715Janoshik2026-Q299.744.60105.7Buyer-sourced0PASS
AX-2026-041552QSC-2605-A6715VendorInvestigate2026-Q299.704.6996.2Buyer-sourced0PASS
AX-2026-041553QSC-2605-A6715VendorInvestigate2026-Q299.934.9592.4Buyer-sourced0PASS
AX-2026-041554QSC-2605-A6715Kestrel2026-Q299.884.85Buyer-sourced0PASS
AX-2026-041555QSC-2605-A6715PeptideMeter2026-Q299.935.2592.1Buyer-sourced0PASS
AX-2026-041556QSC-2605-A6715PeptideMeter2026-Q299.294.30Buyer-sourced0PASS
Other recent GHRP-6 records in the index.
ReportSupplierLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-042012AMBAMB-2603-S5667Janoshik2026-Q399.375.9088.8Laboratory-retained1MARGINAL
AX-2026-042528HJHJ-2603-R5329VendorInvestigate2026-Q398.691.8795.8Buyer-sourced0FAIL
AX-2026-042015AMBAMB-2603-S5667Janoshik2026-Q399.546.4497.1Buyer-sourced0PASS
AX-2026-042526HJHJ-2603-R5329Medutest2026-Q399.373.06Laboratory-retained0PASS
AX-2026-042527HJHJ-2603-R5329VendorInvestigate2026-Q399.212.7793.2Buyer-sourced0PASS
AX-2026-042525HJHJ-2603-R5329Janoshik2026-Q399.523.2492.0Buyer-sourced0PASS
AX-2026-042013AMBAMB-2603-S5667Kestrel2026-Q399.935.75Buyer-sourced0PASS
AX-2026-042017AMBAMB-2603-S5667Medutest2026-Q399.766.4297.4Buyer-sourced0PASS
Other recent QSC records in the index.
ReportCompoundLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-041599CJC-1295 (no DAC)QSC-2606-V7416VendorInvestigate2026-Q397.963.52Buyer-sourced1FAIL
AX-2026-041601CJC-1295 (no DAC)QSC-2606-V7416Kestrel2026-Q398.334.10Buyer-sourced1MARGINAL
AX-2026-041602CJC-1295 (no DAC)QSC-2606-V7416VendorInvestigate2026-Q398.363.38101.8Buyer-sourced1MARGINAL
AX-2026-041477TriptorelinQSC-2607-C5749Nordanalyt2026-Q399.533.42Buyer-sourced0PASS
AX-2026-041600CJC-1295 (no DAC)QSC-2606-V7416Nordanalyt2026-Q397.744.91100.9Buyer-sourced1FAIL
AX-2026-041603CJC-1295 (no DAC)QSC-2606-V7416PeptideMeter2026-Q398.434.20Buyer-sourced1MARGINAL
AX-2026-041606CJC-1295 (no DAC)QSC-2606-V7416Janoshik2026-Q398.033.58Buyer-sourced1MARGINAL
AX-2026-041585LiraglutideQSC-2605-W7381Medutest2026-Q399.595.0992.8Laboratory-retained0PASS