AssayIndex

AX-2026-042529

GHRP-6 · 5 mg declared · Hubei Jianxiang Bioscience Co., Ltd. · lot HJ-2603-R5329

PASSPURITY ONLY
Report ID
AX-2026-042529
Compound
GHRP-6
Compound class
Growth-hormone axis peptides
Supplier
HJ — Hubei Jianxiang Bioscience Co., Ltd.
Batch / lot
HJ-2603-R5329
Declared label claim
5mg
Laboratory
Janoshik Analytical
Assay date
07 Jul 2026
Submitted
25 Jul 2026
Quarter
2026-Q3
Submitter
h.coelho
Sample provenance
Buyer-sourced
Section 1

Results

Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.

ParameterMethodResultUnitIndex spec
PurityRP-HPLC, 30 min gradient, 214 nm99.57% area≥ 99.0PASS
Total impuritiesRP-HPLC, sum of reported peaks0.43% area≤ 1.0PASS
Largest single impurityRP-HPLC — des-Lys (−128 Da)0.21% area≤ 1.00PASS
Identitynot ordered on this submissionnot determinedrequired for VERIFIED statusNOT TESTED
Peptide contentnot ordered on this submissionnot determinedrequired to check label claimNOT TESTED
Water contentKarl Fischer, coulometric, duplicate2.45%≤ 9.0PASS
Counter-ion (acetate)anion-exchange ion chromatography5.99%≤ 12.0PASS
Residual solvent + inorganic residueestimated — see /methods/residual-solvents-q3c/0.68%NOT TESTED
Endotoxinnot ordered on this submissionnot determined≤ 5.0NOT TESTED
Sterilitymembrane filtration, USP <71>, 14 dNo growth at 14 dno growthPASS
Appearancevisual, diffuse light, black and white backgroundWhite cake, partial shrinkage from vial wallwhite to off-white intact cakeFAIL
Reconstitution clarityreconstituted per submitter procedureClear after 90 s gentle swirling, no particulatesclear, no visible particulatesPASS
pH (reconstituted, 1 mg/mL)potentiometric, two-point calibration4.282.5 – 8.0PASS
Retention time (observed)RP-HPLC, 30 min gradient8.69min8.44 ± 0.25 (normalised)PASS
Peak asymmetry (10 % height)Ph. Eur. 2.2.461.300.80 – 1.50PASS
Plate count, main peakN = 5.54 (t/w½)²74,479≥ 20,000PASS
Resolution to nearest impurityvs [D-Trp]-epimer0.92no index criterionREPORTED
Section 2

Chromatogram and peak integration

The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.

031486295944312590 GHRP-68.69 min · 99.57 % 8.47 same trace · ×200 vertical expansion, baseline-corrected · main peak off-scale reporting threshold 0.05 % area 05101520253035 Retention time (min) Response (mAU)
Figure 1. RP-HPLC trace, 30 min gradient, 214 nm. Drawn from the peak-integration table below: peak positions are the reported retention times, peak areas are the reported area percentages, peak widths follow the reported plate count of 74,479, and skew follows the reported asymmetry factor of 1.30. Baseline noise is seeded from the report ID and is illustrative. The lower panel is the same trace at a stated vertical expansion with the slow gradient drift subtracted, because at full scale a 0.21 % impurity against a 99.57 % main peak is a line two pixels tall; the main peak runs off-scale there by design.
#PeakRTArea (µV·s)% areaΔ mass (Da)
1GHRP-6 — main peak8.694,839,41199.57
2des-Lys (−128 Da)8.4710,2070.21-128.095
3oxidised Trp (+16 Da)8.356,8040.14+15.995
4bis-oxidised Trp (+32 Da)8.112,4300.05+31.990
5[D-Trp]-epimer8.571,4580.030.000
Closure check — purity + Σ impurities 100.00CLOSES

Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.

Section 4

Gravimetric mass balance

Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.

Supplier certificate, as declared

The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.

FigureSupplier COAThis reportIndex note
Purity (% area)99.3599.57divergence -0.02 pp vs batch median
Total impurities (% area)0.650.43
Largest single impurity (% area)not stated0.21
Water (%)2.02.45
Counter-ion (%)not stated5.99
Peptide content (%w/w)93.2not determined
Endotoxin (EU/mg)0.31not determined
Method stated on certificateYEScolumn, gradient and wavelength given
Section 5

Provenance and caveats

Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.

Sample provenance
Buyer-sourced
Evidentiary weight
Strongest available evidence in this index.
Chain of custody
Retail purchase → submitter (ambient, 24 d) → laboratory (hand-carried, 9 d) → assay.
Assay date
07 Jul 2026
Submitted to the index
25 Jul 2026
Laboratory
Janoshik Analytical, Ostrava, Czechia
Method basis
30 min gradient · high-resolution MS
Verification status
PURITY ONLY
Section 6

Annotations 2

Signed technical comments from index contributors. Not a discussion forum — annotations question or contextualise the result, and the data team replies where a reply is warranted.

buyer_sourced
Independently purchased, at the submitter's own cost, forwarded without the supplier's involvement. That is the definition and this record meets it.
storage_stated
Ordering under an unremarkable name and address is the whole method. It requires no cooperation from anybody and it produces the strongest evidence this index holds.
Section 7

Related records

Same batch — lot HJ-2603-R5329 n=5

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-042525HJ-2603-R5329Janoshik2026-Q399.523.2492.0Buyer-sourced0PASS
AX-2026-042526HJ-2603-R5329Medutest2026-Q399.373.06Laboratory-retained0PASS
AX-2026-042527HJ-2603-R5329VendorInvestigate2026-Q399.212.7793.2Buyer-sourced0PASS
AX-2026-042528HJ-2603-R5329VendorInvestigate2026-Q398.691.8795.8Buyer-sourced0FAIL
Other recent GHRP-6 records in the index.
ReportSupplierLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-042012AMBAMB-2603-S5667Janoshik2026-Q399.375.9088.8Laboratory-retained1MARGINAL
AX-2026-042528HJHJ-2603-R5329VendorInvestigate2026-Q398.691.8795.8Buyer-sourced0FAIL
AX-2026-042015AMBAMB-2603-S5667Janoshik2026-Q399.546.4497.1Buyer-sourced0PASS
AX-2026-042526HJHJ-2603-R5329Medutest2026-Q399.373.06Laboratory-retained0PASS
AX-2026-042527HJHJ-2603-R5329VendorInvestigate2026-Q399.212.7793.2Buyer-sourced0PASS
AX-2026-042525HJHJ-2603-R5329Janoshik2026-Q399.523.2492.0Buyer-sourced0PASS
AX-2026-042013AMBAMB-2603-S5667Kestrel2026-Q399.935.75Buyer-sourced0PASS
AX-2026-042017AMBAMB-2603-S5667Medutest2026-Q399.766.4297.4Buyer-sourced0PASS
Other recent HJ records in the index.
ReportCompoundLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-042595SemaglutideHJ-2608-C7002Janoshik2026-Q399.503.55Buyer-sourced1MARGINAL
AX-2026-042598SemaglutideHJ-2608-C7002Janoshik2026-Q399.593.84Buyer-sourced0PASS
AX-2026-042605SemaglutideHJ-2608-C7002Janoshik2026-Q399.033.37107.3Buyer-sourced0PASS
AX-2026-042602SemaglutideHJ-2608-C7002Nordanalyt2026-Q399.213.5092.0Buyer-sourced0PASS
AX-2026-042603SemaglutideHJ-2608-C7002Janoshik2026-Q399.163.42105.9Buyer-sourced0PASS
AX-2026-042528GHRP-6HJ-2603-R5329VendorInvestigate2026-Q398.691.8795.8Buyer-sourced0FAIL
AX-2026-042526GHRP-6HJ-2603-R5329Medutest2026-Q399.373.06Laboratory-retained0PASS
AX-2026-042527GHRP-6HJ-2603-R5329VendorInvestigate2026-Q399.212.7793.2Buyer-sourced0PASS